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Thermal Property Testing

Continuously innovating and evolving.

Thermal Characteristics Evaluation

Kguchi evaluates thermal characteristics of materials with the latest equipment, TMA, DSC, and DLF.

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Thermal Expansion Measurement

Thermomechanical Analysis (TMA)

A Thermomechanical Analysis (TMA), is a technique that measures changes in sample size as a function of temperature, time and load. This measurement can detect a change in size from expansion or contraction of the sample as well as a softening or deformation of the sample.

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(Test Method/ Specification)

  • ASTM E1545: Standard Test Method for Assignment of the Glass Transition Temperature by Thermomechanical Analysis
  • ASTM E831: Standard Test Method for Linear Thermal Expansion of Solid Materials by Thermomechanical Analysis
  • ASTM E2347: Standard Test Method for Indentation Softening Temperature by Thermomechanical Analysis ASTM E2092: Standard Test Method for Distortion Temperature in Three-Point Bending by Thermomechanical Analysis

(Equipment)

  • TA Instruments TMAQ400Em
  • Regaku Thermo Plus EvoⅡ

(Material)
Metals, CMCs. Rubber, FRPs

(Temperature Range)
-150℃ to 1000℃

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Determination of Specific Heat Capacity

Determination of Specific Heat Capacity by DSC

Differential Scanning Calorimetry (DSC) is a thermal analysis technique in which the heat flow into or out of a sample is measured as a function of temperature or time, while the sample is exposed to a controlled temperature program.

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(Test Method/ Specification)

  • ISO 8301 Thermal insulation -- Determination of steady-state thermal resistance and related properties -- Heat flow meter apparatus
  • ASTM E 1530 Standard Test Method for Evaluating the Resistance to Thermal Transmission by the Guarded Heat Flow Meter Technique

(Temeprature Range)
20℃ to 100℃

(Material)
heat shield material, foams, CMCs

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Measurement of Thermal Conductivity

Steady-state measurement

The steady-state methods measure thermal properties by establishing a temperature difference that does not change with time.

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(Test Method/ Specification)

  • ISO 8301 Thermal insulation -- Determination of steady-state thermal resistance and related properties -- Heat flow meter apparatus
  • ASTM E 1530 Standard Test Method for Evaluating the Resistance to Thermal Transmission by the Guarded Heat Flow Meter Technique

(Temeprature Range)
20℃ to 100℃

(Material)
heat shield material, foams, CMCs

Laser flash Method

With the Laser-Flash method, the thermal conductivity is determined by the temperature rise in a test sample that is heated by a short laser pulse from one side. The temperature increase caused on the sample surface then propagates as a kind of heat wave through the sample until it is detected on the opposite side by an infrared measuring device.

(Test Method/ Specification)

  • ASTM E1461 Standard Test Method for Thermal Diffusivity by the Flash Method
  • JIS R 1611 Measurement methods of thermal diffusivity, specific heat capacity, and thermal conductivity for fine ceramics by flash method

(Temeprature Range)
20℃ to 1200℃

(Material)
Metals, CMCs. Rubber, FRPs